Jose Manuel Valverde Millán
Professor
e-mail: jmillan@us.es

Education: PhD in Physics, 1997, University of Seville.
Doctoral thesis: Static and dynamics of granular materials Xerographic. Supervisor: Antonio Castellanos Mata y Alberto T. Pérez Izquierdo.

Main scientific results:

Development of a powder test, not only restricted to the diagnosis of fluidity, but also a powerful instrument for investigating the physical properties of cohesive fine powders.
The flow of coarse granular materials is characterized by the transition from plastic to inertial flow, while the flow of fine particles at atmospheric pressure is characterized by the transition from plastic to fluidized flow.
We have developed a powder test, by which the relationship between effort of consolidation, tensile strength and free volume of fine powder, initialized in a reproducible state, is measured.
At low consolidations, the adhesion force between the plastic particles micrometer increase linearly with the load force between particles, indicating the elasto-plastic behavior.
In consolidation stresses greater than 200 Pa, the strength of adhesion between the micrometric plastic particles increase proportionally to the square of the root of the load force between particles, since it corresponds completely to a plastic behavior.
Two regimes have been observed in a non-bubbling fluidised bed of powder Fine: solid and fluidic.
Local measurements of the optical probe show the existence of structures pseudoturbulent mesoscale and short-lived voids in the fluid regime, reminiscent of beds fluidized by liquid, and responsible for rapid diffusive transport.
Fine particles aggregate in DLA fractals aggregated in fluidization due to adhesive forces between particles that exceed several orders of magnitude the particle's weight.
The amount of particles added decreases according to the proportion of force of attraction between particles for the decreases in the weight of the particles.
The range of fluidic behavior in fluidized beds of fine powders decreases as the number of aggregate particles decreases, and tends to zero for particles that are neither coagulable nor aggregated.
The vibration reduces the amplitude of the range of fluidic behavior promoting the rupture of aggregates, therefore the aggregation plays a main role in the prevention of the growth of large bubbles throughout the extended interval of fluid form.
In the transition from fluid to solid, the fractal clusters agglomerate in a metastable state in fractions of volume depending on the attractive energy and close to the volume fraction of unattractive hard spheres in jamming.
Near the phase transition, the stress ratio (solid volume fraction) can be adjusted to a critical functional form for a small range of applied stresses, measured in foams, emulsions and colloidal systems and predicted by numerical simulations in hard spheres.
Above critical stress, the volume-stress ratio of the solid volume passes to the logarithmic law that is typically used to describe the compaction behavior of soils and characterized by a compression index parameter.
The increase of the compression ratio with the proportion of the force of attraction between particles and the weight of the particle is consistent with the hypothesis that the intra-cluster vacuum distribution effectively controls the compaction process.
In the large limit of compaction of our fine irregular particles produced by a wear process reaches a narrow packed package at random with a fraction of particle volume of about 0.54, which is similar to that measured for large mechanically crushed quasimonodisperse grains, such as rocks, of morphology similar to our fine particles.
Avalanche fine cohesive powders through internal sliding surfaces depending on the cohesion of the powder and the boundary conditions, in contrast to the behavior of non-cohesive grains, such as dry sand, where the avalanches consist of surface layers of about ten grains.
In a slowly rotated drum, avalanche sizes, time interval between avalanches and maximum stable angle do not follow a SOC behavior, but scale with powder cohesion.
Avalanches of granular materials of decreasing particle size in a slowly rotated drum shows gradual transition from a coherent oscillation to an irregular long-term correlated behavior reminiscent of the transitional behavior observed in plasmas and reproduced by modified models of cellular automata since the parameter of Fluidization length is increased.
A common observation is that an attractive interaction between particles improves the formation of spatio-temporal structures and, therefore, the memory and collective coherent behavior of the system.

Main scientific publications:
An automated apparatus for measuring the tensile strength and compressibility of fine cohesive powders.Review of Scientific Instruments, Vol. 71, No. 7, July 2000, 2791-2795.

Authors: Jose Manuel Valverde Millán, Antonio Castellanos Mata, Antonio Ramos Reyes, Alberto Tomás Pérez Izquierdo, M.A. Morgan and P. K. Watson.


Flow regimes in fine cohesive powders. Physical Review Letters, vol. 82, issue 6, 1156-1159, February 1999.

Authors: Antonio Castellanos Mata, Jose Manuel Valverde Millán, Alberto Tomás Pérez Izquierdo, Antonio Ramos Reyes and P.K. Watson.


Self-diffusion in a gas-fluidized bed of fine powder. Physical Review Letters, Volume 86, issue 14, 3020-3023, April 2001.

Authors: Jose Manuel Valverde Millán, Miguel Ángel Sánchez Quintanilla, and Antonio Castellanos Mata.


The memory of granular materials. Contemporary Physics, Volume 44, issue 5, 389-399. September 2003.

Authors: Jose Manuel Valverde Millán, Miguel Ángel Sánchez Quintanilla, and Antonio Castellanos Mata.


Jamming threshold of dry fine powders. Physical Review Letters, vol 92, issue 25, 258303, June 2004.

Authors: Jose Manuel Valverde Millán, Miguel Ángel Sánchez Quintanilla, and Antonio Castellanos Mata.



Patents:
1998-11-26.

  • Description: Device and method for measuring cohesion in fine granular media. Patent of Invention.
  • Participants: Valverde Millán, Jose Manuel; Ramos Reyes, Antonio; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 1999-07-01.

  • Description: Device and Procedure for Measuring the Cohesion of Fine Granular Media.
  • Participants: Valverde Millán, Jose Manuel; Ramos Reyes, Antonio; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2005-10-11.

  • Description: Procedure and Device to Measure the Angle of Internal Friction and the Cohesion of Granular Media.
  • Participants: Valverde Millán, Jose Manuel; Sanchez Quintanilla, Miguel Angel; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2006-10-05.

  • Description: Method and device for measuring the angle of friction and the cohesion of granular media.
  • Participants: Valverde Millán, Jose Manuel; Sanchez Quintanilla, Miguel Angel; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2008-07-10.

  • Description: Fluidization of Fine and Ultrafine Powders Assisted by Oscillating Electric Fields.
  • Participants: Valverde Millán, Jose Manuel; Sanchez Quintanilla, Miguel Angel; Espín Milla, Manuel Jesús; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2009-04-30.

  • Description: Assisted Carbon Dioxide Adsorption Procedure.
  • Participants: Valverde Millán, Jose Manuel y Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2009-07-09

  • Description: Fluidization of fine and ultra-fine powders assisted by oscillating electric fields.
  • Participants: Valverde Millán, Jose Manuel; Sanchez Quintanilla, Miguel Angel; Espín Milla, Manuel Jesús; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2011-12-15.

  • Description: Procedure to Improve the Fluidization of Co2 Adsorbent Fine Co2 Adsorbent Powders.
  • Participants: Valverde Millán, Jose Manuel; Soria del Hoyo, Carlos; Espín Milla, Manuel Jesús; Sanchez Quintanilla, Miguel Angel; Castellanos Mata, Antonio.
  • Holder entity: Seville University.
  • 2013-02-22.

  • Description: Method for the capture of CO2 with high temperature, assisted by acoustic vibration.
  • Participants: Valverde Millán, Jose Manuel; Sánchez Quintanilla, Miguel Angel; Pérez Ebri, Jose Manuel
  • Holder entity: Seville University.
  • 2016-04-20.

  • Description: Thermochemical process of concentrated solar energy storage from steel slag.
  • Participants: Valverde Millán, Jose Manuel; Miranda Pizarro, Juan; Perejón, Antonio; Pérez Maqueda, Luis A.; Sánchez Jiménez, Pedro Enrique:
  • Holder entity: Seville University.

  • Popularization books:
    High Solids Redispersion of Liquid Inks.

    Authors: Valverde Millán, Jose Manuel y Castellanos Mata, Antonio.

    Powder Flow: the Shear Fracture of a Tilted Layer of Xerographic Toner. 1997.

    Authors: Ramos Reyes, Antonio; Valverde Millán, Jose Manuel; Castellanos Mata, Antonio; Watson, P. Keith, Watson, P. Keith, et. al.

    Electromagnetic Waves in Anisotropic Dielectric Media. University Editor Group. 2007. ISBN 97-8848-491-847-9.

    Authors: Valverde Millán, Jose Manuel.

    Granular Media Technology. Santander (SPAIN). Secretariat of Publications of the University of Seville. 2008.

    Authors: Valverde Millán, Jose Manuel; Castellanos Mata, Antonio; Sánchez Quintanilla, Miguel Angel.

    Springer Particle Technology Series. Sprin. 2012.

    Authors: Valverde Millán, Jose Manuel.

    Fluidization of Fine Powders: Cohesive versus Dynamical Aggregation. Netherlands. Springer. 2013.

    Authors: Valverde Millán, Jose Manuel.

    Springer Particle Technology Series. Springer. 2012. ISBN 1567-827X.

    Authors: Valverde Millán, Jose Manuel.

    Alternating Field Electronanofluidization. Vol. 1145. Pag. 97-100. En: Powders and Grains 2009: Proceedings of the 6th International Conference on Micromechanics. The American Institute of Physics. 2009. ISBN 978-0-7354-0682-7.

    Authors: Espín Milla, Manuel Jesús; Valverde Millán, Jose Manuel; Sánchez Quintanilla, Miguel Angel; Castellanos Mata, Antonio.

    Magnetofluidization of Fine Magnetite Particles. Vol. 1145. Pag. 119-122. En: Powders and Grains 2009: Proceedings of the 6th International Conference on Micromechanics. The American Institute of Physics. 2009. ISBN 978-0-7354-0682-7.

    Authors: Sánchez Quintanilla, Miguel Angel, Espín Milla, Manuel Jesús; Valverde Millán, Jose Manuel; Castellanos Mata, Antonio.

    Particle Structuring and Yield Stress in Magnetofluidized Beds. Vol. 1254. Pag. 33-38. En: Porous Media and Its Applications in Science, Engineering, and Industry: 3rd International. The American Institute of Physics. 2010. ISBN 978-0-7354-0803-6.

    Authors: Valverde Millán, Jose Manuel; Espín Milla, Manuel Jesús; Sánchez Quintanilla, Miguel Angel; Castellanos Mata, Antonio.



    PhD supervisor:
    Optimization of CO2 capture by fixed and fluidized beds of calcium-based adsorbents at laboratory scale. Doctoral Thesis 2016.

    Author: Pérez Ebrí, Jose Manuel



    For any questions or suggestions contact me through my email.




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